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untitled document
(2020)
The methodology of the approximation and interpretation of thermal desorption spectra (TDS) of hydrogen in some carbon nanostructures and graphite has been developed and applied for such materials.
The methodology is based on a definite approximation by the symmetrical Gaussians of the hydrogen thermal desorption spectra, obtained by using one single heating rate, for carbon materials and nanomaterials, and a definite processing of the Gaussians, in the approximation of the first-order reactions and the second-order ones. It results in determining (with a satisfactory accuracy, for the further physical analysis), from TDS data of one single heating rate, the activation energies and pre-exponential factors of the rate constants of desorption processes corresponding to the main TDS peaks with different temperatures of the maximum desorption rate. The developed methodology contains several successive steps of its implementation, including the use of several “criterions of truth” and the final verification and/or modification of the results, with the help of numerical modeling methods. This technique is not less informative, but much less time-consuming in experimental terms compared to the generally accepted classical Kissinger method, which demands using of several heating rates, and has strict limits of applicability. Furthermore, the methodology allows one to reveal physics and atomic mechanisms of the main desorption processes through thermodynamic analysis of the obtained peak characteristics and comparison with the corresponding independent experimental and theoretical data.
The purpose of such a methodology is to further reveal the weakly studied physics of the main states of hydrogen in carbon materials and nanomaterials, and not the thorough detailed mathematical description of the spectra. For this case, both the large difference and the large spread of the known experimental and theoretical values of the thermodynamic characteristics of the main desorption processes, important for hydrogen storage problems, are also taken into account.
The characteristics and atomic mechanisms (physics) of processes of thermal desorption of deuterium from isotropic graphite at temperatures 700–1700 K are considered.
Due to the good mechanical properties, flax fiber-reinforced epoxy composites
are being widely used as a green alternative to glass fiber composites. However,
plant fibers absorb moisture from the environment, being in a higher moisture
uptake as the relative humidity (RH) increases. This absorbed moisture deteriorates the mechanical properties of the composites. In this study, geometric
and displacement potential function (DPF) approaches are used to predict the
mechanical properties of flax fiber-reinforced epoxy composites under environmental conditions, in particular, different RH values. The tensile properties
that were measured experimentally strongly agreed with the analytical findings.
Almost similar results were found for the tensile strain those were measured
experimentally and the one predicted by the geometric function.
However, the predicted strain values were 38% and 42% less than the experimental ones for 0% and 95% RH conditioned composites, respectively, when
DPF was used. Good conformity between the experimental, analytical, and
DPF formulation for predicting mechanical properties ensures the practical
applicability of this study. The formulations established in this work could,
therefore, be utilized to analytically solve laminated composites under specific
boundary conditions in structural applications.
The moisture absorption behavior of flax fiber-reinforced epoxy composites is deliberated to be a serious issue. This property restricts their usage as outdoor engineering structures. Therefore, this study provides an investigation of moisture in flax fibers on the performance of the flax/epoxy composite materials based on their shear responses. The ±45° aligned flax fibers exposed to different relative humidities (RH) and the vacuum infusion process was used to manufacture the composite specimens. The optimum shear strength (40.25 ± 0.75 MPa) was found for the composites manufactured with 35% RH-conditioned flax fibers, but the shear modulus was reduced consistently with increasing RH values. Although shear strength was increased because of fiber swelling with increased moisture absorption rate until 35% RH environments with good microstructures, nonetheless, strength and modulus both started to decrease after this range. A very poor microstructure has been affirmed by the SEM images of the composite samples conditioned at 90% RH environments.