Metal additive manufacturing of dental prostheses consisting of cobalt−chromium−tungsten (Co−Cr−W) alloys poses an alternative to investment casting. However, metal additive manufacturing processes like Laser Powder‐Bed Fusion (LPBF) can impact the elastic constants and the mechanical anisotropy of the resulting material. To investigate the phase compositions of mechanically different specimens in dependence of their postprocessing steps (e. g. heat treatment to relieve stress), the current study uses X‐ray Diffraction (XRD), Electron BackScatter Diffraction (EBSD), and Transmission Electron Microscopy (TEM) for phase identification. Our studies connect plastic deformation of Remanium star CL alloy with the formation of the hexagonal ϵ‐phase and heat treatment with the formation of the D024‐phase, while partially explaining previously observed differences in Young's moduli.
This paper aims to analyze the stress and strain states appearing in the elbow of a tube, such as those commonly used in a city’s water supply network. The stress field is characterized by the fact that there is a significant stress increase when compared to a straight tube. As a result, the strength of such an elbow must be investigated and guaranteed for such a network to be well designed. A practical solution used is to anchor the elbow in a massive concrete block. The paper compares the stress field that occurs in the elbow when it is free, buried in the ground, and when it is anchored in a massive concrete block. Furthermore, we investigate how a crack appears and propagates in the elbow. This happens especially for the elbow buried in the ground where the stress and strain are higher than when the elbow is anchored in concrete. The results obtained can be used in the current practice in the case of water supply networks made by high-density polyethylene pipes.
Das Interesse der Industrie an additiv gefertigten Bauteilen steigt z unehmend, wobei mit zunehmendem Verständnis der statischen Kennwerte nunmehr der Fokus in Richtung der dynamischen Festigkeiten wandert. Deswegen werden Einflussparameter auf die Lebensdauer und potenzielle Nachbearbeitungsmethoden untersucht und analysiert. Ein großer Einfluss ist dabei der Oberflächengüte und den durch Rautiefen initiierten Kerbeffekten zuzuschreiben. Deswegen werden unterschiedliche Methoden zur Verbesserung der Oberflächengüte untersucht. Dabei werden die Verfahren Laserpolieren, elektrochemisches Polieren und Hartmetallkugelstrahlen und deren Auswirkung auf Oberflächengüte sowie Härte untersucht. Für das elektrochemische Polieren werden die Proben in einer Perchlorsäure für 90 s bei 32 V und maximal 10 A poliert. Das Hartmetallkugelstrahlen wird mit einem UFS 100 Strahlmittel bei einem Druck von 4 bar und einer Strahldauer von 10 s ausgeführt. Anschließend werden Wöhlerlinien für die unterschiedlichen Zustände mittels Umlaufbiegeversuch ermittelt, welche mit Referenzwerten analysierter konventioneller Proben verglichen werden. Des Weiteren werden die Bruchflächen analysiert. Die Untersuchungen ergaben ein hohes Optimierungspotenzial der additiv gefertigten Proben bei einer Verdichtung der Oberfläche sowie einer Entfernung der Randschicht durch eine spanende Bearbeitung. Dadurch wurden höhere Zeitfestigkeiten als mit konventionell gefertigten Proben erreicht.
Additive manufacturing offers unique possibilities to produce complex components, which would not be possible or only very difficult to be realizable with conventional manufacturing processes. The potential of additive manufacturing of aluminum alloys has already been realized in prototyping, but still offers potential in the establishment of series applications. For enabling the establishment of additive manufacturing in series applications, comprehensive knowledge about the material behavior is necessary. This study examines the torsional behavior of additive manufactured AlSi10Mg samples and shows the correlation between tensile and torsional strength. Comprehensive torsion tests with strain gauges were performed and significant directional dependencies were shown. The correlation factor in the area of torsional yield strength/tensile yield strength and torsional strength/tensile strength was determined and was compared with the yield/failure conditions according to Tresca and von Mises.
Laser powder-bed fusion has become one of the most important techniques in additive manufacturing. For guaranteeing the possibility of manufacturing highly specialized and advanced components, currently intensive research is carried out in this field. One area of this research is the material-specific macroscopic anisotropy, which is investigated in our work by comprehensive static mechanical experiments. The material which was tested within this study was the precipitation-hardenable AlSi10Mg alloy, with the focus on installation space orientation. Tensile and compression tests were performed, the results for the Young's modulus in compressive loading exceeded the previously known values of this material in tensile loading and achieved values of up to 79.8 GPa. As a result of this investigation, a chemical spectroscopic analysis was undertaken and from the actual chemical composition, a relative density of 99.86% of the samples was determined.
The methodology of the approximation and interpretation of thermal desorption spectra (TDS) of hydrogen in some carbon nanostructures and graphite has been developed and applied for such materials.
The methodology is based on a definite approximation by the symmetrical Gaussians of the hydrogen thermal desorption spectra, obtained by using one single heating rate, for carbon materials and nanomaterials, and a definite processing of the Gaussians, in the approximation of the first-order reactions and the second-order ones. It results in determining (with a satisfactory accuracy, for the further physical analysis), from TDS data of one single heating rate, the activation energies and pre-exponential factors of the rate constants of desorption processes corresponding to the main TDS peaks with different temperatures of the maximum desorption rate. The developed methodology contains several successive steps of its implementation, including the use of several “criterions of truth” and the final verification and/or modification of the results, with the help of numerical modeling methods. This technique is not less informative, but much less time-consuming in experimental terms compared to the generally accepted classical Kissinger method, which demands using of several heating rates, and has strict limits of applicability. Furthermore, the methodology allows one to reveal physics and atomic mechanisms of the main desorption processes through thermodynamic analysis of the obtained peak characteristics and comparison with the corresponding independent experimental and theoretical data.
The purpose of such a methodology is to further reveal the weakly studied physics of the main states of hydrogen in carbon materials and nanomaterials, and not the thorough detailed mathematical description of the spectra. For this case, both the large difference and the large spread of the known experimental and theoretical values of the thermodynamic characteristics of the main desorption processes, important for hydrogen storage problems, are also taken into account.
The characteristics and atomic mechanisms (physics) of processes of thermal desorption of deuterium from isotropic graphite at temperatures 700–1700 K are considered.
The moisture absorption behavior of flax fiber-reinforced epoxy composites is deliberated to be a serious issue. This property restricts their usage as outdoor engineering structures. Therefore, this study provides an investigation of moisture in flax fibers on the performance of the flax/epoxy composite materials based on their shear responses. The ±45° aligned flax fibers exposed to different relative humidities (RH) and the vacuum infusion process was used to manufacture the composite specimens. The optimum shear strength (40.25 ± 0.75 MPa) was found for the composites manufactured with 35% RH-conditioned flax fibers, but the shear modulus was reduced consistently with increasing RH values. Although shear strength was increased because of fiber swelling with increased moisture absorption rate until 35% RH environments with good microstructures, nonetheless, strength and modulus both started to decrease after this range. A very poor microstructure has been affirmed by the SEM images of the composite samples conditioned at 90% RH environments.